Asmi, Dwi and Sulaiman, Ahmad and Oktavia, Irene L and Badaruddin, Muhammad and Zulfia, Anne (2016) Synthesis and characterisation of composite based biohydroxyapatite bovine bone mandible waste (BHAp) doped with 10 wt % amorphous SiO2 from rice husk by solid state reaction. In: THE 3RD INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS SCIENCE AND TECHNOLOGY (ICAMST 2015),, 6-7 October-2015, Surakarta.
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Abstract
Effect of 10 wt% amorphous SiO2 from rice husk addition on the microstructures of biohydroxyapatite (BHAp) obtained from bovine bone was synthesized by solid state reaction. In this study, biohydroxyapatite powder was obtained from bovine bone mandible waste heat treated at 800 oC for 5 h and amorphous SiO2 powder was extracted from citric acid leaching of rice husk followed by combustion at 700oC for 5 h. The composite powder then mixed and sintered at 1200 oC for 3 h. X-ray diffraction (XRD), Fourier transformed infrared (FTIR) spectroscopy and Scanning electron microscopy (SEM) techniques are utilized to characterize the phase relations, functional group present and morphology of the sample. The study has revealed that the processing procedures played an important role in microstructural development of BHAp-10 wt% SiO2 composite. The XRD study of the raw material revealed that the primary phase material in the heat treated of bovine bone mandible waste is hydroxyapatite and in the combustion of rice husk is amorphous SiO2. However, in the composite the hydroxyapatite, -tricalcium phosphate, and calcium phosphate silicate were observed. The FTIR result show that the hydroxyl stretching band in the composite decrease compared with those of hydroxyapatite spectra and the evolution of morphology was occurred in the composite.
| Item Type: | Conference or Workshop Item (Paper) |
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| Subjects: | Q Science > QC Physics |
| Divisions: | Fakultas Matematika dan Ilmu Pengetahuan Alam (FMIPA) > Prodi Fisika |
| Depositing User: | DWI ASMI |
| Date Deposited: | 13 Jan 2017 01:49 |
| Last Modified: | 13 Jan 2017 01:49 |
| URI: | http://repository.lppm.unila.ac.id/id/eprint/1376 |
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