Bahri, Syaiful and Ambarwati, Yuli and Bayhaqi, Agus and Iqbal, Muhammad Synthesis 4-piperoilmorpholine from piperine.

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Piperine was isolated from black pepper by soxhletation method using technical grade ethanol as a solvent. This compound was used as precursor for the synthesis of 4-piperoilmorpholine. The synthesis was carried out via a pre-target piperoilchloride, where the piperine was initially hydrolyzed using KOH ethanolate for 24 hours, added SOCl2 and then mixed with morpholine at 0-5o C. The result of synthesis was obtained 4-piperoilmorpholine with yield of 40,80%. Keywords: 4-piperoilmorpholine, piperine, soxhletation, hydrolysis

Item Type: Article
Subjects: Q Science > QD Chemistry
Divisions: Fakultas Matematika dan Ilmu Pengetahuan Alam (FMIPA) > Prodi Kimia
Depositing User: Syaiful Bahri
Date Deposited: 29 May 2020 13:54
Last Modified: 29 May 2020 13:54

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