Lestari, Anggun and Ginting, Simparmin and Saputra, Hens (2019) Effect of Seed Amounts on the Synthesis of Zeolite ZSM-5 Using Coal Bottom Ash and Rice Husk as Sources of Silica and Alumina by Using Seeding Method. Materials Science Forum, 948 (1). pp. 9-13. ISSN 1662-9752

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Official URL: doi:10.4028/www.scientific.net/MSF.948.9

Abstract

ZSM-5 has been successfully synthesized by seeding method using coal bottom ash and rice husk as the sources of silica and alumina.Synthesis ZSM-5 were performed by the hydrothermal method in autoclave autogenous at 180 ˚C for 36 h with molar ratio 10Na : 50SiO : 2Al2O3 : 500H2O with the addition of ZSM-5 commercial as seed. In this experiments, investigated variations seed amounts of 5, 10, 15, and 20% of weight silica. The product was characterized using X-Ray Diffraction (XRD), Fourier Transform Infrared (FTIR), Scanning Electron Microscope (SEM), and Brunauer-Emmet-Teller (BET). Resulted showed that ZSM-5 succeed formed in all variation of seed contain. At variation seed amount 5%, crystallinity obtained still low in which content of quartz phase still be high. Percent crystallinity highest obtained at the variation of seed amount 20% with the result percent crystallinity relative 106%. The experimental results revealed that phase transformation has occurred, in which an amorphous phase of coal bottom ash and rice husk has been transformed to the ZSM-5 crystal with addition seed as substitution organic template.

Item Type: Article
Subjects: T Technology > TP Chemical technology
Divisions: Fakultas Teknik (FT) > Prodi Teknik Kimia
Depositing User: SIMPARMIN
Date Deposited: 21 May 2019 03:04
Last Modified: 21 May 2019 03:04
URI: http://repository.lppm.unila.ac.id/id/eprint/13068

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